3CIJ
Crystal structure of A. fulgidus periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Collection date | 2007-03-22 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.901, 75.396, 116.996 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.070 |
R-free | 0.14930 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | SHELX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.070 |
Number of reflections | 285208 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.4 | 293 | 30mM Tris pH 8.4, 0.16M Na2SO4, 5% glycerol, 28% PEG 4K, sitting drop at 293K. , VAPOR DIFFUSION, SITTING DROP |