3CG1
Crystal structure of P. furiosus periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2007-09-16 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.21340 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.460, 109.790, 55.430 |
Unit cell angles | 90.00, 96.22, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
Rwork | 0.186 |
R-free | 0.20460 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.700 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 140430 | |
Completeness [%] | 97.7 | 93.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | Bicine, NaCl, PEG 600, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |