3CFZ

Crystal structure of M. jannaschii periplasmic binding protein ModA/WtpA with bound tungstate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2007-05-18
Detector	PSI PILATUS 6M
Wavelength(s)	1.21420
Spacegroup name	P 21 21 21
Unit cell lengths	37.880, 89.589, 97.868
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.700
Rwork	0.185
R-free	0.20040
Structure solution method	SAD
RMSD bond length	0.012
RMSD bond angle	1.600
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.700	1.700
Number of reflections	68998
Completeness [%]	97.4	93.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	7		Ammonium Chloride, PEG 3350, pH 7.0, VAPOR DIFFUSION