3CFX
Crystal structure of M. acetivorans periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2007-07-29 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.21440 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 115.500, 51.860, 124.048 |
| Unit cell angles | 90.00, 116.93, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.600 |
| Rwork | 0.210 |
| R-free | 0.23530 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.700 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 1.600 | 1.600 |
| Number of reflections | 165102 | |
| Completeness [%] | 97.5 | 93.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | MES, Magnesium Acetate, PEG 8000, pH 6.5, VAPOR DIFFUSION, temperature 293K |
