3CFX
Crystal structure of M. acetivorans periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2007-07-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.21440 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.500, 51.860, 124.048 |
Unit cell angles | 90.00, 116.93, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
Rwork | 0.210 |
R-free | 0.23530 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.700 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 165102 | |
Completeness [%] | 97.5 | 93.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | MES, Magnesium Acetate, PEG 8000, pH 6.5, VAPOR DIFFUSION, temperature 293K |