3CCH
H-2Db complex with murine gp100
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2007-03-04 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.934 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.500, 176.600, 85.500 |
Unit cell angles | 90.00, 120.00, 90.00 |
Refinement procedure
Resolution | 19.600 - 2.600 |
R-factor | 0.24266 |
Rwork | 0.241 |
R-free | 0.27859 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.475 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.600 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 65171 | |
Completeness [%] | 96.4 | 89.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 277 | 1.8M Ammonium Sulfate, 0.1M Tris, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |