Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-12-02 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97931 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 39.738, 77.271, 80.044 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.870 - 1.700 |
| R-factor | 0.19079 |
| Rwork | 0.190 |
| R-free | 0.21470 |
| Structure solution method | SAD |
| RMSD bond length | 0.030 |
| RMSD bond angle | 1.448 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXCD |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.700 |
| High resolution limit [Å] | 1.610 | 1.610 |
| Rmerge | 0.047 | 0.329 |
| Number of reflections | 31979 | |
| <I/σ(I)> | 33.65 | 2.7 |
| Completeness [%] | 97.0 | 96.6 |
| Redundancy | 5.7 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.1 | 295 | 0.2M Mg Acetate, 20% PEG 3350, Cryoprotected in paratone-N oil, pH 5.1, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
