3C7Y
Mutant R96A OF T4 lysozyme in wildtype background at 298K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1998-05-07 |
Detector | SDMS |
Wavelength(s) | 1.5414 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 61.039, 61.039, 97.092 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.000 - 1.950 |
R-factor | 0.211 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l63 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.410 |
Data reduction software | san (Deigo Multiwire) |
Data scaling software | San (Deigo Multiwire) |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.000 | 1.980 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.080 | |
Number of reflections | 14074 | |
Completeness [%] | 89.0 | 83.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 277 | 2 M NA/K PHOSPHATE PH 6.7 550 mM NACL 50 MM REDUCED BME, 50 MM OXIDIZED BME , VAPOR DIFFUSION, HANGING DROP, temperature 277K |