3C1D
X-ray crystal structure of RecX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-05-17 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97940 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.549, 71.757, 74.657 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.500 - 1.800 |
R-factor | 0.182 |
Rwork | 0.180 |
R-free | 0.22300 |
Structure solution method | MAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.327 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.500 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.556 |
Number of reflections | 28281 | |
<I/σ(I)> | 7.2 | 1.4 |
Completeness [%] | 98.7 | 98 |
Redundancy | 6.9 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | 15% PEG 4000, 0.2 M Sodium Acetate, 0.1 M Tris-Cl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291.0K |