3C07
Crystal structure of a TetR family transcriptional regulator from Streptomyces coelicolor A3(2)
Replaces: 2OFLExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97931 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 74.947, 74.947, 208.075 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.250 - 2.700 |
R-factor | 0.22116 |
Rwork | 0.218 |
R-free | 0.28894 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.891 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | SHELXD |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.250 | 2.780 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.096 | 0.867 |
Number of reflections | 17068 | |
<I/σ(I)> | 54.57 | 3.5 |
Completeness [%] | 99.5 | 100 |
Redundancy | 18.1 | 16 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 1.5 Ammonium sulfate, 0.1M Tris-HCl, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |