3BZ5
Functional domain of InlJ from Listeria monocytogenes includes a cysteine ladder
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-27 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.817 |
Spacegroup name | I 2 3 |
Unit cell lengths | 159.272, 159.272, 159.272 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.280 - 2.700 |
R-factor | 0.18512 |
Rwork | 0.182 |
R-free | 0.25261 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o6v |
RMSD bond length | 0.022 |
RMSD bond angle | 1.815 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.280 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.112 | 0.391 |
Number of reflections | 18486 | |
<I/σ(I)> | 17.9 | 5.3 |
Completeness [%] | 99.9 | |
Redundancy | 11.2 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 298 | 2M Ammonium sulfate, 0.1M Na acetate, pH 4.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |