3BYR
Mode of Action of a Putative Zinc Transporter CzrB (Zn form)
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F2 |
Synchrotron site | CHESS |
Beamline | F2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-02 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.2827, 1.2818, 1.2567 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.750, 74.560, 43.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.430 - 1.800 |
R-factor | 0.209 |
Rwork | 0.207 |
R-free | 0.25000 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.109 |
Data reduction software | DPS |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.3.0021) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 7849 | |
<I/σ(I)> | 20.1 | 4.6 |
Completeness [%] | 98.2 | 96.4 |
Redundancy | 7.3 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 277 | 28 mg/ml protein, 25 mM zinc chloride, 0.1 M Tris-Hcl, pH 7.50, BATCH, temperature 277K |