3BXL

Crystal structure of the R-type calcium channeL (CaV2.3) IQ domain and CA2+calmodulin complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Detector technology	IMAGE PLATE
Collection date	2006-10-07
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.54178
Spacegroup name	I 41 2 2
Unit cell lengths	124.606, 124.606, 74.024
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.300
R-factor	0.20768
Rwork	0.205
R-free	0.26162
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.098
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.300
Number of reflections	12496

Crystallization Conditions

crystal ID	method	pH	temperature	details
1