3BXK
Crystal structure of the P/Q-type calcium channel (CaV2.1) IQ domain and CA2+calmodulin complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Collection date | 2006-10-28 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 80.655, 80.431, 63.837 |
| Unit cell angles | 90.00, 97.56, 90.00 |
Refinement procedure
| Resolution | 24.870 - 2.550 |
| R-factor | 0.2157 |
| Rwork | 0.213 |
| R-free | 0.26703 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.232 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 13241 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
