3BP3
Crystal structure of EIIB
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Detector technology | CCD |
| Collection date | 2006-04-21 |
| Wavelength(s) | 0.97884, 0.97901, 0.97121 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 108.193, 108.149, 28.947 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.760 - 1.650 |
| R-factor | 0.213 |
| Rwork | 0.213 |
| R-free | 0.24100 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.200 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.760 |
| High resolution limit [Å] | 1.650 |
| Number of reflections | 19901 |
| Completeness [%] | 94.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
