3BOI
Snow Flea Antifreeze Protein Racemate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-B |
| Synchrotron site | APS |
| Beamline | 23-ID-B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-07 |
| Detector | MARRESEARCH |
| Spacegroup name | P -1 |
| Unit cell lengths | 28.603, 32.404, 59.849 |
| Unit cell angles | 88.69, 89.18, 73.41 |
Refinement procedure
| Resolution | 25.000 - 1.000 |
| R-factor | 0.219 |
| Rwork | 0.218 |
| R-free | 0.23300 |
| Starting model (for MR) | 3b0g |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.613 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 0.980 |
| High resolution limit [Å] | 0.950 | 0.950 |
| Rmerge | 0.084 | 0.420 |
| Number of reflections | 101192 | |
| <I/σ(I)> | 17.4 | 3.6 |
| Completeness [%] | 78.2 | 18.9 |
| Redundancy | 4.3 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
