3BJ1
met-Perch Hemoglobin at pH 5.7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 93 |
Detector technology | CCD |
Detector | MAR CCD 130 mm |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.225, 84.780, 121.905 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.670 - 1.900 |
R-factor | 0.18707 |
Rwork | 0.185 |
R-free | 0.22989 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ouu |
RMSD bond length | 0.017 |
RMSD bond angle | 1.550 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 69.670 |
High resolution limit [Å] | 1.800 |
Number of reflections | 44493 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |