3B0B
Crystal structure of the chicken CENP-S/CENP-X complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9642, 0.97944, 0.97889, 0.9951 |
Spacegroup name | P 61 |
Unit cell lengths | 48.741, 48.741, 345.633 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.211 - 2.150 |
R-factor | 0.1901 |
Rwork | 0.186 |
R-free | 0.23480 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.959 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.211 | 2.230 |
High resolution limit [Å] | 2.150 | 2.150 |
Number of reflections | 25152 | |
Completeness [%] | 99.7 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 9.5 | 293 | 100mM Citrate-BisPropane pH 9.5, 500mM NaCl, 100mM MgSO4, and 30% PEG 600, VAPOR DIFFUSION, temperature 293K |
1 | VAPOR DIFFUSION | 9.5 | 293 | 100mM Citrate-BisPropane pH 9.5, 500mM NaCl, 100mM MgSO4, and 30% PEG 600, VAPOR DIFFUSION, temperature 293K |