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3AZJ

Crystal Structure of Human Nucleosome Core Particle Containing H4K44Q mutation

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2009-11-23
DetectorADSC QUANTUM 315
Wavelength(s)1.0000
Spacegroup nameP 21 21 21
Unit cell lengths105.955, 109.428, 180.904
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.610 - 2.890
Rwork0.220
R-free0.26800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2cv5
RMSD bond length0.008
RMSD bond angle1.300
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.950
High resolution limit [Å]2.8902.900
Number of reflections47901
<I/σ(I)>4.5
Completeness [%]99.9100
Redundancy7.37.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6293POTASSIUM CACODYLATE, POTASSIUM CHLORIDE, MANGANESE CHLORIDE, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K

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