3AZ7
Crystal structure of Pt/T-HEWL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-03-08 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.412, 78.412, 36.558 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.310 - 2.100 |
R-factor | 0.2233 |
Rwork | 0.219 |
R-free | 0.30322 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.018 |
RMSD bond angle | 1.633 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (6.1.13) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.061 | 0.281 |
Number of reflections | 7077 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 26.9 | 27 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | Sodium chloride, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 100K, temperature 293K |