3AZ4
Crystal structure of Co/O-HEWL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.154, 55.473, 71.928 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.330 - 1.620 |
R-factor | 0.21613 |
Rwork | 0.215 |
R-free | 0.24633 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bgi |
RMSD bond length | 0.009 |
RMSD bond angle | 1.189 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (6.1.13) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.650 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmerge | 0.027 | 0.296 |
Number of reflections | 15911 | |
Completeness [%] | 99.0 | 100 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 300 | Sodium chloride, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 300K |