3AW7
Crystal structure of tetragonal hen egg white lysozyme at 71.9% relative humidity
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU ULTRAX 18 |
Temperature [K] | 300.6 |
Detector technology | IMAGE PLATE |
Collection date | 2009-11-09 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.247, 78.247, 37.331 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.920 - 2.100 |
R-factor | 0.16286 |
Rwork | 0.160 |
R-free | 0.21805 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3aw6 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.585 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.046 | 0.254 |
Number of reflections | 6466 | |
<I/σ(I)> | 20.8 | 3.3 |
Completeness [%] | 90.1 | 86.7 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 293 | 3-8%(w/v) NaCl, 100mM Na acetate, pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |