3AUY
Crystal structure of Rad50 bound to ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2010-03-12 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.160, 95.300, 110.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.400 - 2.700 |
R-factor | 0.228 |
Rwork | 0.228 |
R-free | 0.29600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ii8 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.300 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.300 | 2.720 |
High resolution limit [Å] | 2.630 | 2.630 |
Number of reflections | 24959 | |
Completeness [%] | 98.8 | 99.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 9.5% PEG 8000, 0.1M sodium cacodylate pH6.5, 0.1M magnessium acetate, 1mM ADP, VAPOR DIFFUSION, HANGING DROP, temperature 295.0K |