3AUW
Cytoplasmic domain of inward rectifier potassium channel Kir3.2 in complex with cadmium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-02-06 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1.00000 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 100.808, 100.808, 105.812 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 3.560 |
R-factor | 0.2865 |
Rwork | 0.281 |
R-free | 0.33110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.763 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.560 |
Rmerge | 0.206 |
Number of reflections | 26865 |
<I/σ(I)> | 6.714 |
Completeness [%] | 99.0 |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |