3ATY
Crystal structure of TcOYE
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-07-04 |
| Detector | RIGAKU RAXIS V |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.291, 78.791, 78.797 |
| Unit cell angles | 90.00, 93.37, 90.00 |
Refinement procedure
| Resolution | 45.750 - 1.700 |
| R-factor | 0.17 |
| Rwork | 0.170 |
| R-free | 0.19500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.300 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Number of reflections | 75469 | |
| Completeness [%] | 100.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | PEG 1500, Ammonium fluoride, urea, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
