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3AR4

Calcium pump crystal structure with bound ATP and TG in the absence of Ca2+

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2007-04-16
DetectorADSC QUANTUM 315
Wavelength(s)0.9
Spacegroup nameP 41 21 2
Unit cell lengths71.381, 71.381, 590.690
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution14.970 - 2.150
R-factor0.239
Rwork0.239
R-free0.28100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1AGV
RMSD bond length0.007
RMSD bond angle1.300
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]100.0002.200
High resolution limit [Å]2.1502.150
Rmerge0.0560.394
Number of reflections83710
<I/σ(I)>21.93.13
Completeness [%]99.199.7
Redundancy7.85.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICRODIALYSIS6.1283pH 6.1, MICRODIALYSIS, temperature 283K
1MICRODIALYSIS6.1283pH 6.1, MICRODIALYSIS, temperature 283K

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