3AR2
Calcium pump crystal structure with bound AMPPCP and Ca2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-12-20 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 0.75 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 161.995, 75.306, 151.541 |
Unit cell angles | 90.00, 108.97, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.500 |
R-factor | 0.24817 |
Rwork | 0.247 |
R-free | 0.27243 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zbd |
RMSD bond length | 0.009 |
RMSD bond angle | 1.252 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.560 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 59761 | |
<I/σ(I)> | 31.8 | 2.7 |
Completeness [%] | 99.8 | 98.5 |
Redundancy | 3.3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 6.1 | 283 | pH 6.1, MICRODIALYSIS, temperature 283K |