3AQB
M. luteus B-P 26 heterodimeric hexaprenyl diphosphate synthase in complex with magnesium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2008-03-07 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | I 21 3 |
Unit cell lengths | 189.613, 189.613, 189.613 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.400 |
R-factor | 0.24134 |
Rwork | 0.240 |
R-free | 0.27564 |
Structure solution method | SIRAS |
RMSD bond length | 0.003 |
RMSD bond angle | 0.616 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 133.630 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 44225 | |
<I/σ(I)> | 29.3 | 5.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.4 | 11.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 0.08M Tris-HCl (pH 8.5), 0.16M Magnesium chloride hexahydrate, 24% (w/v) PEG 4000, 20% (v/v) Glycerol, VAPOR DIFFUSION, SITTING DROP, temperature 277K |