3ANA
THREE-DIMENSIONAL STRUCTURE OF D(GGGATCCC) IN THE CRYSTALLINE STATE
Experimental procedure
Detector technology | DIFFRACTOMETER |
Detector | STOE |
Spacegroup name | P 61 |
Unit cell lengths | 46.830, 46.830, 44.490 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.500 |
R-factor | 0.166 |
RMSD bond length | 0.040 |
RMSD bond angle | 0.034 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 |
Rmerge | 0.029 * |
Total number of observations | 1594 * |
Number of reflections | 1300 * |
Completeness [%] | 78.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 7.5 * | MICRODIALYSIS |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | DNA | 4 (mM) | ||
2 | 1 | 2 | 24 (%(v/v)) | ||
3 | 1 | sodium cacodylate | 20 (mM) | ||
4 | 1 | magnesium chloride | 5 (mM) |