3ALR
Crystal structure of Nanos
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 63 |
Unit cell lengths | 100.961, 100.961, 71.577 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.100 |
R-factor | 0.16527 |
Rwork | 0.163 |
R-free | 0.20787 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.477 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.6.0046) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.082 | 0.300 |
Number of reflections | 23796 | |
<I/σ(I)> | 15.7 | 5.1 |
Completeness [%] | 97.7 | 80.5 |
Redundancy | 10.3 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Sodium Formate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |