3AG1

Bovine Heart Cytochrome c Oxidase in the Carbon Monoxide-bound Fully Reduced State at 280 K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	280
Collection date	2004-11-28
Wavelength(s)	0.9
Spacegroup name	P 21 21 21
Unit cell lengths	189.493, 210.887, 178.301
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 2.200
Rwork	0.162
R-free	0.19200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2eij
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.3)

Data quality characteristics

	Overall
Low resolution limit [Å]	94.900
High resolution limit [Å]	2.200
Number of reflections	353208

Crystallization Conditions

crystal ID	method	pH	temperature	details
1