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3A8U

Crystal Structure of omega-Amino Acid:Pyruvate Aminotransferase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-18B
Synchrotron sitePhoton Factory
BeamlineBL-18B
Temperature [K]287
Detector technologyIMAGE PLATE
Collection date1995-04-12
DetectorRIGAKU
Wavelength(s)1.0
Spacegroup nameI 2 2 2
Unit cell lengths124.460, 137.790, 61.570
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 1.400
R-factor0.14675
Rwork0.146
R-free0.15763
Structure solution methodMIR
RMSD bond length0.010
RMSD bond angle1.341
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.9001.190
High resolution limit [Å]1.1501.150
Rmerge0.0320.773
Number of reflections135011
<I/σ(I)>210.26
Completeness [%]73.617.6
Redundancy1317.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Dialysis7.82772.2M ammonium sulphate, 0.33M potassium phosphate buffer, pH 7.8, Dialysis, temperature 277K

222036

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