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3A6U

Crystal structure of MutT-8-OXO-dGMP-MN(II) complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL40B2
Synchrotron siteSPring-8
BeamlineBL40B2
Temperature [K]100
Detector technologyCCD
Collection date2003-04-24
DetectorADSC QUANTUM 4
Wavelength(s)1.2906
Spacegroup nameP 21 21 21
Unit cell lengths38.234, 56.003, 59.339
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution18.200 - 2.560
R-factor0.193
Rwork0.193
R-free0.24200
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)3a6t
RMSD bond length0.007
RMSD bond angle1.300
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]18.5602.720
High resolution limit [Å]2.5602.560
Rmerge0.0770.152
Number of reflections4395
<I/σ(I)>45.922.6
Completeness [%]99.295.7
Redundancy6.03
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.62882.0M AMMONIUM SULFATE, 0.2M POTASSIUM SODIUM TARTRATE, 0.1M TRISODIUM CITRATE, pH 5.60, VAPOR DIFFUSION, HANGING DROP, temperature 288K
1VAPOR DIFFUSION, HANGING DROP5.62882.0M AMMONIUM SULFATE, 0.2M POTASSIUM SODIUM TARTRATE, 0.1M TRISODIUM CITRATE, pH 5.60, VAPOR DIFFUSION, HANGING DROP, temperature 288K

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