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3A5J

Crystal structure of protein-tyrosine phosphatase 1B

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]98
Detector technologyCCD
Collection date2008-11-18
DetectorADSC QUANTUM 315
Wavelength(s)1.000
Spacegroup nameP 32 2 1
Unit cell lengths88.426, 88.426, 72.467
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution26.880 - 1.700
R-factor0.18995
Rwork0.188
R-free0.22857
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2cma
RMSD bond length0.025
RMSD bond angle2.180
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.760
High resolution limit [Å]1.7001.700
Rmerge0.0510.252
Number of reflections36101
<I/σ(I)>38.47.75
Completeness [%]98.993.6
Redundancy10.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROPVAPOR DIFFUSION, HANGING DROP

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