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3A44

Crystal structure of HypA in the dimeric form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]100
Detector technologyCCD
Collection date2008-10-24
DetectorADSC QUANTUM 270
Wavelength(s)1.0000
Spacegroup nameP 21 21 21
Unit cell lengths56.830, 97.975, 136.480
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.160 - 3.310
R-factor0.292
Rwork0.292
R-free0.33700
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3a43
RMSD bond length0.016
RMSD bond angle1.700
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.420
High resolution limit [Å]3.3003.300
Number of reflections11039
<I/σ(I)>16.72.1
Completeness [%]92.863.7
Redundancy6.14.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52930.1M Tris-HCl, pH8.5, 24% PEG8000, 22% isopropanol, VAPOR DIFFUSION, SITTING DROP, temperature 293K

224004

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