3A34
Effect of Ariginine on lysozyme
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU ULTRAX 18 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-07-15 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 78.357, 78.357, 37.312 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 33.690 - 1.650 |
| R-factor | 0.19718 |
| Rwork | 0.196 |
| R-free | 0.22589 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1hel |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.967 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.690 | 1.740 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.048 | 0.107 |
| Number of reflections | 13045 | |
| <I/σ(I)> | 6.5 | |
| Completeness [%] | 48.7 | |
| Redundancy | 6.4 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
