3ZO5

Structure of SENP2-Loop1 in complex with preSUMO-2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	H 3 2
Unit cell lengths	145.518, 145.518, 104.671
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	80.520 - 2.150
R-factor	0.19041
Rwork	0.188
R-free	0.23627
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2io0
RMSD bond length	0.020
RMSD bond angle	2.337
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.330	2.260
High resolution limit [Å]	2.150	2.150
Rmerge	0.040	0.770
Number of reflections	23228
<I/σ(I)>	21	2.2
Completeness [%]	99.8	99.2
Redundancy	5.1	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1