3ZG6

The novel de-long chain fatty acid function of human sirt6

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Spacegroup name	H 3 2
Unit cell lengths	104.891, 104.891, 231.492
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	35.730 - 2.200
R-factor	0.19343
Rwork	0.191
R-free	0.23581
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.024
RMSD bond angle	2.207
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.240
High resolution limit [Å]	2.200	2.200
Rmerge	0.060
Number of reflections	25066
<I/σ(I)>	47.9	4.7
Completeness [%]	99.8	100
Redundancy	10.8	11

Crystallization Conditions

crystal ID	method	pH	temperature	details
1