3WMR
Crystal structure of VinJ
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-11-07 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 52.870, 72.620, 75.450 |
| Unit cell angles | 114.02, 98.39, 98.50 |
Refinement procedure
| Resolution | 50.960 - 1.950 |
| R-factor | 0.16737 |
| Rwork | 0.165 |
| R-free | 0.20576 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3nwo |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.214 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.960 | 2.000 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Number of reflections | 63636 | |
| Completeness [%] | 88.7 | 65.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 278 | 0.2M lithium acetate, 20% polyethylene glycol 3350, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 278K |
