3WMP
Crystal structure of SLL-2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-06-15 |
| Detector | ADSC QUANTUM 270 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.030, 189.950, 57.050 |
| Unit cell angles | 90.00, 110.55, 90.00 |
Refinement procedure
| Resolution | 94.980 - 2.000 |
| R-factor | 0.251 |
| Rwork | 0.251 |
| R-free | 0.27100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ccv |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.400 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 2.030 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 69338 | |
| Completeness [%] | 99.4 | 98.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 293 | MPD, calcium formate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
