3WIK
Crystal structure of the CK2alpha/compound10 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2011-11-11 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.90 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.382, 79.451, 82.888 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.785 - 1.995 |
R-factor | 0.1656 |
Rwork | 0.163 |
R-free | 0.21140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.852 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 57.030 |
High resolution limit [Å] | 1.850 |
Number of reflections | 27524 |
Completeness [%] | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 25% ethyleneglycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K |