3WHJ
Crystal structure of Nas2 N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Detector technology | CCD |
Collection date | 2012-08-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97946 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 64.590, 64.590, 149.760 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.650 |
R-factor | 0.161 |
Rwork | 0.159 |
R-free | 0.19700 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.571 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.088 | 0.391 |
Number of reflections | 23180 | |
<I/σ(I)> | 45.7 | 4.4 |
Completeness [%] | 99.8 | 100 |
Redundancy | 10 | 10.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.9M sodium acetate trihydrate, 0.1M HEPES (pH 8.5), 50mM cadmium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |