3WAR
Crystal structure of human CK2a
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2010-10-16 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 51.454, 78.313, 80.136 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 56.000 - 1.040 |
| R-factor | 0.14458 |
| Rwork | 0.143 |
| R-free | 0.16751 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.031 |
| RMSD bond angle | 2.243 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 56.000 |
| High resolution limit [Å] | 1.040 |
| Number of reflections | 141117 |
| Completeness [%] | 91.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 25% ethylene glycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
