3W9U
Crystal structure of Lipk107
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-06-24 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.075 |
| Spacegroup name | P 32 |
| Unit cell lengths | 65.484, 65.484, 63.871 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 50.000 - 2.000 |
| R-factor | 0.18124 |
| Rwork | 0.179 |
| R-free | 0.21473 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ex9 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.049 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 56.700 | 2.030 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 19653 | |
| Completeness [%] | 95.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | Sodium citrate, PEG4000,2-propanol, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
