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3W2V

Crystal structure of the Cmr2dHD-Cmr3 subcomplex bound to 3'-AMP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]95
Detector technologyCCD
Collection date2012-10-22
DetectorADSC QUANTUM 270
Wavelength(s)0.98
Spacegroup nameI 2 2 2
Unit cell lengths103.940, 136.669, 191.973
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution41.730 - 2.600
R-factor0.215
Rwork0.215
R-free0.25900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3ung
RMSD bond length0.007
RMSD bond angle1.300
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareCNS (1.3)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.640
High resolution limit [Å]2.6002.600
Rmerge0.0630.063
Number of reflections42206
Completeness [%]99.799.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP629312.5-15% 2-propanaol, 18mM MgCl2, 45mM MES (pH 6.0), 20mM ammonium acetate, 10mM sodium acetate, 3% PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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