3VXC
Crystal Structure of Xylobiose-BxlE complex from Streptomyces thermoviolaceus OPC-520
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS VII |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 103.672, 163.157, 42.931 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.810 - 1.850 |
R-factor | 0.17026 |
Rwork | 0.168 |
R-free | 0.21282 |
Structure solution method | MAD |
RMSD bond length | 0.023 |
RMSD bond angle | 1.816 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.000 |
High resolution limit [Å] | 1.780 |
Rmerge | 0.071 |
Number of reflections | 69417 |
Completeness [%] | 98.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 3.2 | 293 | 25% PEG 3350, 0.1M citrate, 15% glycerol, pH 3.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 3.2 | 293 | 25% PEG 3350, 0.1M citrate, 15% glycerol, pH 3.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |