3VLB

Crystal structure of xeg-edgp

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Detector technology	CCD
Collection date	2011-05-20
Detector	RAYONIX MX225HE
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	249.043, 51.691, 143.235
Unit cell angles	90.00, 122.21, 90.00

Refinement procedure

Resolution	10.000 - 2.700
R-factor	0.26167
Rwork	0.257
R-free	0.34075
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3vl8 3vla
RMSD bond length	0.014
RMSD bond angle	1.537
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.700
Number of reflections	40308

Crystallization Conditions

crystal ID	method	pH	temperature	details
1