3TWD
glmuC1 in complex with an antibacterial inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E+ DW |
| Spacegroup name | P 63 |
| Unit cell lengths | 80.526, 80.526, 139.850 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 69.840 - 1.900 |
| R-free | 0.21730 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.396 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.3.0034) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 69.840 |
| High resolution limit [Å] | 1.900 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 19-22% (w/v) PEG3350, 100mM PCTP pH 5.5 and 400mM ammonium sulfate, VAPOR DIFFUSION, HANGING DROP |
