3TN2
structure analysis of MIP1-beta P8A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9793 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 51.062, 36.972, 31.061 |
| Unit cell angles | 90.00, 108.54, 90.00 |
Refinement procedure
| Resolution | 29.450 - 1.600 |
| R-factor | 0.15927 |
| Rwork | 0.157 |
| R-free | 0.19909 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.023 |
| RMSD bond angle | 2.074 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 1.600 | 1.600 |
| Number of reflections | 6611 | |
| Completeness [%] | 95.2 | 95.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 5.5 | 298 | 15% v/v ethanol, 0.1 M MES, pH 5.5, 0.2 M zinc acetate, EVAPORATION, temperature 298K |
