3SUA
Crystal structure of the intracellular domain of Plexin-B1 in complex with Rac1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Wavelength(s) | 0.9763 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 142.340, 224.250, 258.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.810 - 4.390 |
R-factor | 0.2351 |
Rwork | 0.234 |
R-free | 0.26380 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.160 |
Refinement software | BUSTER (2.9.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 4.390 |
Number of reflections | 25525 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |