Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 31-ID |
| Synchrotron site | APS |
| Beamline | 31-ID |
| Detector technology | CCD |
| Collection date | 2010-01-01 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 133.046, 73.236, 138.023 |
| Unit cell angles | 90.00, 96.80, 90.00 |
Refinement procedure
| Resolution | 22.100 - 2.100 |
| R-factor | 0.2272 |
| Rwork | 0.225 |
| R-free | 0.27190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.509 |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 22.100 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 147820 |
| Completeness [%] | 95.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Sitting Batch | 7.2 | 298 | PEG 8000, pH 7.2, Sitting Batch, temperature 298K |
